P-Chiral thioxaphosphoranesulphenyl chlorides [RR1P(S)SCI](R =L-menthoxy, R1= EtO) are synthesized in high yield and with optical purity, they are shown to undergo nucleophilic attack at the dico-ordinate sulphur centre by a synchronous mechanism.
A. Lopusiński, L. Luczak and J. Michalski, J. Chem. Soc., Chem. Commun., 1989, 1694 DOI: 10.1039/C39890001694
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