Preparative electrochemical oxidation of metallated phenyl prenyl sulphone leads to a previously unknown cyclic dimer, the formation of which has been rationalized, providing strong evidence for a radical-anion coupling mechanism in outer-sphere oxidative dimerization of α-sulphonyl carbanions.
C. Amatore, A. Thiebault and J. Verpeaux, J. Chem. Soc., Chem. Commun., 1989, 1543 DOI: 10.1039/C39890001543
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