A method for the efficient detection and chemical shift determination of the insensitive 103Rh nucleus via31P detected indirect two-dimensional 31P, 103Rh{1H} n.m.r. is elaborated and its usefulness for rapid access to some new 103Rh n.m.r. data of RhI compounds is demonstrated.
C. J. Elsevier, J. M. Ernsting and W. G. J. de Lange, J. Chem. Soc., Chem. Commun., 1989, 585 DOI: 10.1039/C39890000585
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