The yields of the 16-membered-ring intramolecular cycloaddition products, β-truxinate (4) and δ-truxinate (5), can be greatly increased by making use of the hydrophobic or entropy-driven forces in aggregating media.
X. Jiang, Y. Hui and Z. Fei, J. Chem. Soc., Chem. Commun., 1988, 689 DOI: 10.1039/C39880000689
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