(+)-Malyngolide (+)-(1), the antipode of natural malyngolide, was synthesized in 9 steps from dimethyl (2R,3R)-(–)-tartrate acetonide (3)via(2R)-(–)-2-nonylbutane-1,2,4-triol (8) in 5.1 % overall yield.
Y. Tokunaga, H. Nagano and M. Shiota, J. Chem. Soc., Perkin Trans. 1, 1986, 581 DOI: 10.1039/P19860000581
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