Polyacetylene and polypyrrole, conjugated polymers, were treated with a TCNE–AlCl3–benzene solution and converted into conducting meterials, leading to the formation of partial electron transfer π-complexes and to the substitution of TCNE onto the pyrrole rings, as shown by e.s.r. and 13C n.m.r. spectroscopy.
I. Kulszewicz-Bajer and D. Billaud, J. Chem. Soc., Chem. Commun., 1986, 1720 DOI: 10.1039/C39860001720
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