The thermal decomposition of trimethyloxonium hexachloroantimonate and tetrafluoroborate has been studied in the 50–350°C temperature range; C–C bond formation was only observed at high temperatures in the chlorine-containing system under radical-type reaction conditions.
P. Rimmelin, A. Brenner, K. Fischer and J. Sommer, J. Chem. Soc., Chem. Commun., 1986, 1497 DOI: 10.1039/C39860001497
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