The number and type of hydroxy groups on a TiO2 surface can be determined using a combination of wet chemical techniques, F– exchange, OH– and Fe(acac)3(Hacac = pentane-2,4-dione) adsorption, and i.r. spectroscopy.
J. A. R. van Veen, F. T. G. Veltmaat and G. Jonkers, J. Chem. Soc., Chem. Commun., 1985, 1656 DOI: 10.1039/C39850001656
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