SCHEDULED MAINTENANCE:
1,3-Bis(dimethylamino)isoquinolines(1a–d) dimerise in the presence of silver perchlorate to yield the C-protonated diperchlorates (2a–d), which are irreversibly deprotonated to the corresponding hindered 4,4′-bi-isoquinolyls (3a–d); the dimerisation also occurs by cyclic voltammetry.
G. V. Boyd, O. Hammerich, P. F. Lindley, J. C. Mitchell, G. A. Nicolaou and A. R. Walton, J. Chem. Soc., Chem. Commun., 1985, 885 DOI: 10.1039/C39850000885
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