Highly Stereoselective addition of dithiane anions with 2-methyl-3-trimethylsilylbut-3-enal combined with the stereoselective addition of Grignard reagents to chiral α-alkoxyketones affords a practical and efficient method for the construction of the title compounds.
A. K. Samaddar, T. Chiba, Y. Kobayashi and F. Sato, J. Chem. Soc., Chem. Commun., 1985, 329 DOI: 10.1039/C39850000329
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