Five-co-ordinate complexes [Nu2SiMe2H]+X–; Nu = 3-methyl-1-imidazolio, N,N-dimethylaminopyridinio, or pyridinio; X = Cl, I, or OSO2CF3, have been identified in solution by 29Si n.m.r. spectroscopy, and in some cases isolated as analytically pure compounds.
A. R. Bassindale and T. Stout, J. Chem. Soc., Chem. Commun., 1984, 1387 DOI: 10.1039/C39840001387
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