Synthesis of both (R)-and (S)-2-methyl-3-trimethylsilylbut-3-enal (1), and the preparation of the four possible steric isomers of β-methylhomoally alcohols (2) ans (3) using (1) is decribed.
Y. Kobayashi, Y. Kitano and F. Sato, J. Chem. Soc., Chem. Commun., 1984, 1329 DOI: 10.1039/C39840001329
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