The X-ray structure determination of the title compound, obtained by recrystallisation of LiC(PMe2)3 from pentane–tetrahydrofuran (thf) as colourless crystals, reveals it to be dimeric with two nearly planar (Me2P)3C-moieties linked by (thf)Li fragments via chelating and additional π-type interactions.
H. H. Karsch and G. Müller, J. Chem. Soc., Chem. Commun., 1984, 569 DOI: 10.1039/C39840000569
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