A double five-ring silicate has been identified for the first time in the ZSM-5 synthesis mixture using 29Si n.m.r., attenuated total reflection Fourier transform-infrared spectroscopy, and mass spectrometry; a redistribution of the silicate species present in the solution phase has been observed after the addition of organic solvents to the ZSM-5 synthesis mixture.
G. Boxhoorn, O. Sudmeijer and P. H. G. van Kasteren, J. Chem. Soc., Chem. Commun., 1983, 1416 DOI: 10.1039/C39830001416
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