Synthesis of cyclobutanocrown ethers by intramolecular photocycloaddition
Abstract
Irradiation of divinyloxy compounds {CH2
CHOCH2[CH2OCH2]NCH2OCH
CH2; n= 1–4} in the presence of 1,4-dicyanonaphthalene in benzene gave cis- and trans-cyclobutanocrown ethers in good yields.
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