The crystal structure and absolute configuration of one of the isomers of (+)K[Co(L-valinato)2(CO3)] has been determined, and shown to be Λ(+)-cis(N)-cis(O)-K[Co(L-valinato)2δδ(CO3)]·2H2O. The crystals are orthorhombic, space group P212121, with a= 21.41, b= 14.68, c= 5.76 Å, and Z= 4. The structure has been refined to R= 0.087 for 996 reflections.
M. G. Price and D. R. Russell, J. Chem. Soc., Dalton Trans., 1981, 1067 DOI: 10.1039/DT9810001067
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