An X-ray analysis of [Ni9S9(PEt3)6][BPh4]2 shows that the nine nickel atoms in the [Ni9S9(PEt3)6]2+ cluster lie in a confacial bi-octahedral arrangement and are held together by bridging sulphur atoms, while six phosphine groups complete the co-ordination around the nickel atoms.
C. A. Ghilardi, S. Midollini and L. Sacconi, J. Chem. Soc., Chem. Commun., 1981, 47 DOI: 10.1039/C39810000047
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