The suppression of cyclisation side reactions during silicate derivatisation by the method of Tamás et al., using dimethylformamide as solvent, is demonstrated; the cyclic nature of the silicate skeleton in Pb2SiO4 is confirmed.
L. S. D. Glasser and E. E. Lachowski, J. Chem. Soc., Chem. Commun., 1980, 973 DOI: 10.1039/C39800000973
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