U.v. photolysis of diacyl disulphides gives acylthiyl radicals [RC(O)S·] which react with alkenes, trialkyl phosphites, and dialkyl sulphides to give adducts which have been detected by e.s.r. spectroscopy.
J. R. M. Giles and B. P. Roberts, J. Chem. Soc., Chem. Commun., 1980, 62 DOI: 10.1039/C39800000062
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