Oximes, O-acyl-oximes, and O-alkyl-oximes were reduced with pyridine–borane in the presence of acid to the corresponding hydroxylamine derivatives without over-reduction. Unstable O-acyl-hydroxylamines were directly synthesized for the first time from the corresponding O-acyl-oximes.
M. Kawase and Y. Kikugawa, J. Chem. Soc., Perkin Trans. 1, 1979, 643 DOI: 10.1039/P19790000643
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