Reaction of arenediazonium ions with [Fe(CO)L2(η4-polyene)][L = CO or P(OMe)3, polyene = cyclo-octatetraene or cycloheptatriene], and subsequent deprotonation gives either azo-coupled or arylated compounds such as [Fe(CO){P(OMe)3}2(η4-C8H7N2C6H4F-p)] and [Fe(CO)3(η4-C8H7C6H4NO2-p)] respectively.
N. G. Connelly, A. R. Lucy and M. W. Whiteley, J. Chem. Soc., Chem. Commun., 1979, 985 DOI: 10.1039/C39790000985
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