N-(Diphenylphosphinyl)hydroxylamine (4a) can be prepared from diphenylphosphinic chloride using O-trimethylsilylhydroxylamine; it forms O-acetyl (5a) and O-methanesulphonyl (6a) derivatives, the latter undergoing Lossen-like rearrangement in t-butylamine.
M. J. P. Harger, J. Chem. Soc., Chem. Commun., 1979, 930 DOI: 10.1039/C39790000930
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