Electron diffraction studies show that methylated derivatives of hydroxylamine exist in two conformations differing by a 180° rotation about the N–O bond, as predicted by M.O. calculations, but with a much smaller free energy difference than the calculations would suggest.
F. G. Riddell, E. S. Turner, D. W. H. Rankin and M. R. Todd, J. Chem. Soc., Chem. Commun., 1979, 72 DOI: 10.1039/C39790000072
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