The first acylfluorophosphorane, Ph2PF2[C(:O)Ph], has been isolated from the reaction of Ph2POEt with benzoyl fluoride; the X-ray structure determination proved that the acyl group occupies an equatorial position at trigonal-bipyramidal phosphorus.
S. Neumann, D. Schomburg, G. Richtarsky and R. Schmutzler, J. Chem. Soc., Chem. Commun., 1978, 946 DOI: 10.1039/C39780000946
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