A single-step synthesis of 4,6,8,11,13,15,19,21,23,26,28,30-dodecamethyl-1,2,16,17-tetrathia[2.1.2.1]metacyclophane is reported. The structure of this compound was determined by reductive degradation to bis-(3-mercaptomesityl)methane and reoxidation of the latter to the original macrocycle, and by mass spectrometry.
F. Bottino, S. Foti and S. Pappalardo, J. Chem. Soc., Perkin Trans. 1, 1977, 1652 DOI: 10.1039/P19770001652
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