Aryl compounds containing a variety of heteroatomic substituents give good yields of the corresponding perchloro-derivatives when treated with a mixture of sulphur monochloride and anhydrous aluminium chloride in sulphuryl chloride solution; in aryl fluorides, such as hexafluorobenzene, considerable replacement of fluorine by chlorine takes place.
C. Glidewell and J. C. Walton, J. Chem. Soc., Chem. Commun., 1977, 915 DOI: 10.1039/C39770000915
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