By observing the isotopic chemical shifts when OH groups are replaced by OD under conditions of low exchange rate, it is possible to differentiate hydroxy-bearing carbon atoms in carbohydrates using 13C n.m.r. spectroscopy at 62·8 MHz.
D. Gagnaire and M. Vincendon, J. Chem. Soc., Chem. Commun., 1977, 509 DOI: 10.1039/C39770000509
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