Photochemical bromination of methyl tri-O-acetyl-2,6-anhydro-L-gulonate (2) with N-bromosuccinimide gives methyl tri-O-acetyl-α-L-xylo-hexulopyranosylonate bromide (5) which, on acetoxylation and hydrolysis, provides a further synthetic route to L-ascorbic acid.
R. J. Ferrier and R. H. Furneaux, J. Chem. Soc., Chem. Commun., 1977, 332 DOI: 10.1039/C39770000332
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