An X-ray diffraction analysis of the CCl4 clathrate of the mercapto-host (II) is described; a key feature of the host structure is the linking of the SH groups of six molecules of (II) by SH ⋯ S hydrogen bonds, such that the sulphur atoms form a near-planar hexagon.
A. D. U. Hardy, D. D. MacNicol, J. J. McKendrick and D. R. Wilson, J. Chem. Soc., Chem. Commun., 1977, 292 DOI: 10.1039/C39770000292
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