The diaxial isomer (II) of 6,7-di-iodobicyclo-[3.1.1]heptane has been prepared by addition of iodine to tricyclo[4.1.0.02,7]heptane; the structure of (II), which does not undergo substitution by carbon nucleophiles, has been determined by single crystal X-ray diffraction.
S. Mazur, A. H. Schroder and M. C. Weiss, J. Chem. Soc., Chem. Commun., 1977, 262 DOI: 10.1039/C39770000262
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