Crystals of [Rh(NO)(SO2)(PPh3)2] have been obtained from SO2-saturated solutions of Rh(NO)(PPh3)3 in benzene–heptane mixtures; the X-ray crystal structure shows the SO2 ligand co-ordinated to the rhodium through the sulphur atom and through one of the oxygen atoms, while the RhNO angle is 140°.
D. C. Moody and R. R. Ryan, J. Chem. Soc., Chem. Commun., 1976, 503b DOI: 10.1039/C3976000503B
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