Dimethyl hemiorthoformate has been shown to be an intermediate in the hydrolysis of acetoxydimethoxymethane in a mixture of [2H6]acetone (9 vols.) and deuterium oxide (1 vol.) at –35 °C and its formation and decomposition have been studied by following the changes in the n.m.r. spectrum.
B. Capon, J. H. Gall and D. McL. A. Grieve, J. Chem. Soc., Chem. Commun., 1976, 1034 DOI: 10.1039/C39760001034
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