Oxidation of 2,2,6,6-tetramethylpiperidin-4-ol (1a) with m-chloroperbenzoic acid in methylene chloride produces, in addition to the expected nitroxide (1b), varying amounts of 4-oxo-2,2,6,6-tetramethylpiperidin-1-oxyl (2).
J. A. Cella, J. A. Kelley and E. F. Kenehan, J. Chem. Soc., Chem. Commun., 1974, 943a DOI: 10.1039/C3974000943A
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