Thermal decomposition of N-(1,1-dimethylprop-2-ynyl)-N-t-butylaminoxyl (2) gives 9-isopropylidene-3,3-dimethyl-5,8-di-t-butyl-5,8-diaza-4,7-dioxabicyclo [4,2,1]-nonan-2-one (3) as the major product whose molecular structure was determined by X-ray crystallography.
R. L. Craig, J. Murray-Rust, P. Murray-Rust and J. S. Roberts, J. Chem. Soc., Chem. Commun., 1973, 751 DOI: 10.1039/C39730000751
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