Substitution of [2,2]metacyclophane (1) with out transannular bonding has been performed using BzO·OBz–CuCl2–MeCN, to produce the 4-benzoate (3a) and the 8-cyanomethyl derivative (4).
T. Sato and K. Nishiyama, J. Chem. Soc., Chem. Commun., 1973, 220 DOI: 10.1039/C39730000220
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