The formation of thia [5,5]cyclophanes from carbonyl compounds and aromatic dithiols has been re-investigated. The synthetic procedure was improved and crystalline thiacyclophane oligomers were also isolated. N.m.r. and u.v. data of the thiacyclophanes were obtained and their usefulness in determining the structures is discussed.
R. E. Busby and D. Huckle, J. Chem. Soc., Perkin Trans. 1, 1972, 1705 DOI: 10.1039/P19720001705
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