A Fourier Transform method has been used to measure the longitudinal relaxation times of the anomeric protons of eight anomeric pairs of pyranose derivatives; in every instance the axial proton has a shorter relaxation time than its equatorial counterpart.
L. D. Hall and C. Preston, J. Chem. Soc., Chem. Commun., 1972, 1319 DOI: 10.1039/C39720001319
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