The synthesis is reported of 3-(4-methoxy-phenyl)propionic acid (11) asymmetrically labelled at C-3 with deuterium by a procedure which involves as key step the palladium-catalysed ring opening of the optically active oxazine (6).
C. Fuganti, D. Ghiringhelli and P. Grasselli, J. Chem. Soc., Chem. Commun., 1972, 1152 DOI: 10.1039/C39720001152
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