Acid-catalysed cyclization of γ-hydroperoxy-alcohols (2) into 1,2,4-trioxepans (3), a novel class of seven-membered ring peroxide heterocycles, and their mass spectral fragmentation is described.
W. Adam and N. Duran, J. Chem. Soc., Chem. Commun., 1972, 798 DOI: 10.1039/C39720000798
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