Methyl polyfluoroalkyl sulphides, synthesised by two novel routes: (i) photochemical reaction of a polyfluoroiodoalkane with dimethyl sulphide or dimethyl disulphide and (ii) reaction of a polyfluoroiodoalkane with sodium methanethiolate in the presence of dimethyl disulphide, are useful precursors of polyfluoroalkane-sulphonic acids.
R. N. Haszeldine, B. Hewitson, B. Higginbottom, R. B. Rigby and A. E. Tipping, J. Chem. Soc., Chem. Commun., 1972, 249 DOI: 10.1039/C39720000249
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