Methyl crepenynate has been synthesised from non-3-yn-1-yl-triphenylphosphonium bromide (obtained from hept-1-yne via non-3-yn-1-ol and 1-bromonon-3-yne) and the C9 aldehyde-ester with butyl-lithiumin ether, and from it crepenynic acid was obtained by alkaline hydrolysis.
R. W. Bradshaw, A. C. Day, E. R. H. Jones, C. B. Page, V. Thaller and R. A. V. Hodge, J. Chem. Soc. C, 1971, 1156 DOI: 10.1039/J39710001156
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