Dodeca-2,3-dien-1-ol was synthesised by the reductive elimination of the tetrahydropyran-2′-yloxy group from 4-tetrahydropyran-2′-yloxydodec-2-yn-1-ol, and oxidised with active manganese dioxide to the corresponding allenic aldehyde which, on treatment with the anion of trimethyl phosphonoacetate, gave (±)-methyl tetradeca-trans-2,4,5-trienoate.
P. D. Landor, S. R. Landor and S. Mukasa, J. Chem. Soc. D, 1971, 1638 DOI: 10.1039/C29710001638
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