2-Adamantyl methanesulphonate has been converted by pyrolysis in 95% yield into a mixture (2 : 3) of protoadamantene (4) and 2,4-dehydroadamantane (5); hydroboration of protoadamantene and oxidation afforded protoadamantan-4- and -5-ones (5 : 4).
J. Boyd and K. H. Overton, J. Chem. Soc. D, 1971, 211 DOI: 10.1039/C29710000211
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