Treatment of Co2(CO)8 with and excess of NO in hexane solution results in the formation of Co(NO)2NO2 which has been characterized by an X-ray crystal structure determination and by i.r. studies in the solid state and in solution.
C. E. Strouse and B. I. Swanson, J. Chem. Soc. D, 1971, 55 DOI: 10.1039/C29710000055
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