Synthesis of some trimeric sulphanuric compounds: methylsulphanuric dichloride, bis(dichlorophenyl)sulphanuric chloride, di(n-octylamino)- and bis(diethylamino)sulphanuric fluorides

Abstract

Methylsulphanuric dichloride and diphenylsulphanuric chloride were prepared from sulphuric chloride using dimethyl- and diphenyl-mercury; the substituted phenyl compound was obtained by chlorination. The disubstituted sulphanuric fluorides were obtained by the action of excess base on the trifluoride. Infrared spectra and nomenclature are discussed.