A general stereospecific synthesis of hydrind-4-en-2-ones is described in which the 1-mono-ester of a cyclohex-3-ene-1,2-diol is converted by a variant of the Claisen rearrangement into a cyclohex-3-ene-1,2-diacetic acid, which is then cyclised.
I. J. Bolton, R. G. Harrison and B. Lythgoe, J. Chem. Soc. D, 1970, 1512b DOI: 10.1039/C2970001512B
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