The catalytic decomposition of bis-α-diazoketones, in inert solvents, under the high dilution conditions of Ruggli–Ziegler, affords cycloalk-2-ene-1,4-diones; the method was applied to the synthesis of 4-hydroxytropone (γ-tropolone).
J. Font, F. Serratosa and J. Valls, J. Chem. Soc. D, 1970, 721 DOI: 10.1039/C29700000721
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