In the reaction between lead tetra-acetate and a series of substituted acetophenone oximes in methylene chloride, three types of stable nitrogen free radical are observed. Two of these are unambiguously assigned structures of the iminoxy and acetoxy-phenylethane nitroso radical anions. The reaction between these oximes and lead tetra-acetate is sensitive to substituent and steric hindrance effects.
J. W. Lown, J. Chem. Soc. B, 1966, 644 DOI: 10.1039/J29660000644
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