An adiabatic method for studying exothermic solid reactions has been developed. Adiabatic conditions can be maintained in samples of a few grams weight for rates of temperature rise from 2–150 deg./min. The adiabatic decomposition of NH4ClO4 has been studied in the temperature range from 240–325°C.
S. H. Inami, W. A. Rosser and H. Wise, Trans. Faraday Soc., 1966, 62, 723 DOI: 10.1039/TF9666200723
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