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Issue 3, 2017
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An automated repeating batch with catalyst recycle approach to nitro group hydrogenolysis

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Abstract

An automated repeating batch approach has been developed for the rapid screening and scale up of a nitroaromatic to aniline catalytic hydrogenolysis. Advantages of this approach include the ability to scale up in small equipment using readily available powdered catalysts, rapid reaction kinetics due to high catalyst to substrate ratio, lower overall catalyst use, high throughput from a small reactor, and the ability to refresh the catalyst without manual intervention.

Graphical abstract: An automated repeating batch with catalyst recycle approach to nitro group hydrogenolysis

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Supplementary files

Article information


Submitted
04 Jan 2017
Accepted
13 Feb 2017
First published
13 Feb 2017

React. Chem. Eng., 2017,2, 288-294
Article type
Communication

An automated repeating batch with catalyst recycle approach to nitro group hydrogenolysis

K. P. Cole, M. D. Johnson, M. E. Laurila and J. R. Stout, React. Chem. Eng., 2017, 2, 288 DOI: 10.1039/C7RE00002B

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